dodecaphenyl pentastannane

Base Information

Chemical Name:dodecaphenyl pentastannane
CAS No.:13400-08-3
Molecular Formula:C₇₂H₆₀Sn₅
Molecular Weight:1518.82
Hs Code.:

Synonyms:dodecaphenyl pentastannane

Suppliers and Price of dodecaphenyl pentastannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dodecaphenyl pentastannane

Chemical Property:

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Technology Process of dodecaphenyl pentastannane

There total 6 articles about dodecaphenyl pentastannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1011-95-6
diphenyltin

: 1091-26-5
methoxytriphenylstannane

: 1065-93-6
(C₆H₅)3Sn{Sn(C₆H₅)2}nSn(C₆H₅)3

: {(C₆H₅)3Sn}2{Sn(C₆H₅)2}2

: 1064-10-4
hexaphenylditin

: 13400-08-3
dodecaphenyl pentastannane

Guidance literature:: In not given; reaction at 20°C;;

Reference yield:

: phenylmagnesium bromide

: 13400-08-3
dodecaphenyl pentastannane

Guidance literature:: With diethyl ether;

Reference yield:

: 2[Sn(Sn(C₆H₅)3)3]^(1-)*Ca⁽²⁺⁾=Ca[Sn(Sn(C₆H₅)3)3]2

: 639-58-7
triphenyltin chloride

: 4554-93-2,13400-08-3
tetrakis (triphenylstannyl) tin

Guidance literature:: In tetrahydrofuran; byproducts: CaCl2; (N2); using Schlenk techniques; dropwise addn. of soln. of Ph3SnCl in THF to cooled (-60°C) soln. of Ca(Sn(SnPh3)3)2 in THF; stirring for4 h; warming to room temp., removal of solvent in vac., addn. of Et2O/n-hexane (1:1); filtration; removal of solvent in vac., recrystn. from 1:1 mixt. of toluene and Et2O; elem. anal.;
DOI:10.1016/S0022-328X(00)00440-X