4,4-diphenylcyclohexanone oxime

Base Information

Chemical Name:4,4-diphenylcyclohexanone oxime
CAS No.:35380-17-7
Molecular Formula:C₁₈H₁₉NO
Molecular Weight:265.355
Hs Code.:

Synonyms:4,4-diphenylcyclohexanone oxime

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Chemical Property of 4,4-diphenylcyclohexanone oxime

Chemical Property:

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Technology Process of 4,4-diphenylcyclohexanone oxime

There total 1 articles about 4,4-diphenylcyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4528-68-1
4,4-diphenylcyclohexan-1-one

: 35380-17-7
4,4-diphenylcyclohexanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 20 ℃; for 2h;
DOI:10.1021/ol035564x

Reference yield: 28.0%

: 35380-17-7
4,4-diphenylcyclohexanone oxime

: 615268-45-6
1-chloro-1-nitro-4,4-diphenylcyclohexane

Guidance literature:: With trichloroisocyanuric acid; sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃; for 24h;
DOI:10.1021/ol035564x

Reference yield:

: 35380-17-7
4,4-diphenylcyclohexanone oxime

: 2-(4',4'-diphenylcyclohexyl)-tetrahydrofuran

Guidance literature:: Multi-step reaction with 6 steps

1.1: 28 percent / trichloroisocyanuric acid; NaHCO₃ / H₂O; ethyl acetate / 24 h / 20 °C

2.1: 48 percent / NaBH₄ / Pd/C / ethanol / 1 h / 20 °C

3.1: 50 percent / NaOH; cetyl ammonium bromide / tetrahydrofuran; H₂O / 12 h / 20 °C

4.1: 62 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / 1.33 h / cooling

5.1: 87 percent / (S)-(-)-α,α-diphenyl-2-pyrrolidinemethanol; borane dimethyl sulfide complex / tetrahydrofuran / 0.83 h / Heating

6.1: DMAP / CH₂Cl₂ / 20 °C

6.2: HF / acetonitrile; H₂O / 0.08 h / 20 °C

6.3: 25 percent / AIBN; tributyltin hydride / benzene / 12 h / Heating

With dmap; sodium hydroxide; sodium tetrahydroborate; oxalyl dichloride; (S)-diphenylprolinol; dimethylsulfide borane complex; trichloroisocyanuric acid; cetyl ammonium bromide; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; 3.1: Henry reaction / 4.1: Swern oxidation;
DOI:10.1016/j.tet.2006.03.063