1-nitro-4,4-diphenylcyclohexane

Base Information

Chemical Name:1-nitro-4,4-diphenylcyclohexane
CAS No.:615268-46-7
Molecular Formula:C₁₈H₁₉NO₂
Molecular Weight:281.354
Hs Code.:

Synonyms:1-nitro-4,4-diphenylcyclohexane

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Chemical Property of 1-nitro-4,4-diphenylcyclohexane

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Technology Process of 1-nitro-4,4-diphenylcyclohexane

There total 3 articles about 1-nitro-4,4-diphenylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 615268-45-6
1-chloro-1-nitro-4,4-diphenylcyclohexane

: 615268-46-7
1-nitro-4,4-diphenylcyclohexane

Guidance literature:: With sodium tetrahydroborate; palladium on activated charcoal; In ethanol; at 20 ℃; for 1h;
DOI:10.1021/ol035564x DOI:10.1016/j.tet.2006.03.063

Reference yield:

: 4528-68-1
4,4-diphenylcyclohexan-1-one

: 615268-46-7
1-nitro-4,4-diphenylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / hydroxylamine hydrochloride; sodium acetate / ethanol; H₂O / 2 h / 20 °C

2: 28 percent / trichloroisocyanuric acid; NaHCO₃ / H₂O; ethyl acetate / 24 h / 20 °C

3: 48 percent / NaBH₄ / Pd/C / ethanol / 1 h / 20 °C

With sodium tetrahydroborate; trichloroisocyanuric acid; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water; ethyl acetate;
DOI:10.1016/j.tet.2006.03.063

Reference yield:

: 35380-17-7
4,4-diphenylcyclohexanone oxime

: 615268-46-7
1-nitro-4,4-diphenylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / trichloroisocyanuric acid; NaHCO₃ / H₂O; ethyl acetate / 24 h / 20 °C

2: 48 percent / NaBH₄ / Pd/C / ethanol / 1 h / 20 °C

With sodium tetrahydroborate; trichloroisocyanuric acid; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water; ethyl acetate;
DOI:10.1016/j.tet.2006.03.063