N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

Base Information

Chemical Name:N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide
CAS No.:374593-76-7
Molecular Formula:C₂₃H₂₁NO₄S
Molecular Weight:407.49
Hs Code.:

Synonyms:N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

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Chemical Property of N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

Chemical Property:

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Technology Process of N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

There total 4 articles about N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 374593-75-6
N-(3,4-methylenedioxyphenyl)methyl-3-methoxyaminobenzene

: 374593-76-7
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 20h;
DOI:10.1248/cpb.49.1132

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 374593-76-7
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Ti(i-PrO)4 / 3 h / 80 °C

1.2: 99 percent / NaBH₄ / methanol / 1 h / 20 °C

2.1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

With titanium(IV) isopropylate; triethylamine; In benzene;
DOI:10.1248/cpb.49.1132

Reference yield:

: 103-04-8
(phenylthio)acetic acid

: 374593-76-7
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / 1 h / 20 °C

2: 22.6 g / Et₃N / benzene / 20 h / 20 °C

With oxalyl dichloride; triethylamine; In benzene;
DOI:10.1248/cpb.49.1132