BiCl(C₆H₃(CH₂N(CH₃)2)2)2

Base Information

Chemical Name:BiCl(C₆H₃(CH₂N(CH₃)2)2)2
CAS No.:882031-96-1
Molecular Formula:C₂₄H₃₈BiClN₄
Molecular Weight:627.026
Hs Code.:

BiCl(C<sub>6</sub>H<sub>3</sub>(CH<sub>2</sub>N(CH<sub>3</sub>)2)2)2

Synonyms:BiCl(C₆H₃(CH₂N(CH₃)2)2)2

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Chemical Property of BiCl(C₆H₃(CH₂N(CH₃)2)2)2

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Technology Process of BiCl(C₆H₃(CH₂N(CH₃)2)2)2

There total 1 articles about BiCl(C₆H₃(CH₂N(CH₃)2)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 19851-44-6
1,3-bis[(dimethylamino)methyl]benzene

: 7787-60-2
bismuth(III) chloride

: 882031-96-1
BiCl(C₆H₃(CH₂N(CH₃)2)2)2

Guidance literature:: With butyllithium; In diethyl ether; under Ar atm. soln. BuLi in hexane was added to soln. 1,3-(Me2NCH2)2C6H4in hexane, stirred under reflux for 12 h, siolvent was removed in vacuo , residue was dissolved in Et2O and added dropwise at -80°C to soln. BiCl3 in Et2O, 12 h at room temp.; soln. was filtered and evapd.;
DOI:10.1021/ic052160n

Reference yield: 87.0%

: 882031-96-1
BiCl(C₆H₃(CH₂N(CH₃)2)2)2

: C₁₂H₁₉N₂Se⁽¹⁺⁾*Cl^(1-)

: C₂₀H₂₆BiCl₂^(1-)*C₁₂H₁₉N₂Se⁽¹⁺⁾

Guidance literature:: In acetonitrile; for 24h;
DOI:10.1039/c3dt52886c

Reference yield: 67.0%

: 882031-96-1
BiCl(C₆H₃(CH₂N(CH₃)2)2)2

: 882031-93-8
2,6-bis(dimethylaminomethyl)phenyldibismuthane

Guidance literature:: With magnesium; 1,2-dibromoethane; In tetrahydrofuran; under Ar atm. soln. Bi complex in THF was added at -20°C to Mg activated with 1,2-dibromoethane and stirred for 3 h, warmed to 10°C; solvent was removed in vacuo, residue was extd. with petroleum ether andfiltered, solvent was removed in vacuo;
DOI:10.1021/ic052160n