benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

Base Information

Chemical Name:benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate
CAS No.:849114-68-7
Molecular Formula:C₃₀H₄₇N₇O₁₄
Molecular Weight:729.742
Hs Code.:

Synonyms:benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

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Chemical Property of benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

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Technology Process of benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

There total 5 articles about benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 849114-67-6
benzyl N-tris{[2-(2,3,4,5,6-pentachlorophenoxycarbonyl)ethoxy]methyl}methyl carbamate

: (N-hydroxy-N-methylcarbamoylmethyl)ammonium 2,2,2-trifluoroacetate

: 849114-68-7
benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 96h;
DOI:10.1016/j.bmc.2004.11.053

Reference yield:

: 220431-66-3
benzyl N-{tris[2-(ethoxycarbonyl)ethoxymethyl]methyl}carbamate

: 849114-68-7
benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / ethanol; H₂O / 0 °C

2: 72 percent / 4-(dimethylamino)pyridine; DCC / tetrahydrofuran / 48 h / 20 °C

3: 49 percent / triethylamine / tetrahydrofuran / 96 h / 20 °C

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.bmc.2004.11.053

Reference yield:

: 132491-90-8
3-[2-Amino-3-(2-ethoxycarbonyl-ethoxy)-2-(2-ethoxycarbonyl-ethoxymethyl)-propoxy]-propionic acid ethyl ester

: 849114-68-7
benzyl N-tris{[2-[((N-hydroxy-N-methylcarbamoyl)methyl)aminocarbonyl]ethoxy]methyl}methylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dioxane

2: NaOH / ethanol; H₂O / 0 °C

3: 72 percent / 4-(dimethylamino)pyridine; DCC / tetrahydrofuran / 48 h / 20 °C

4: 49 percent / triethylamine / tetrahydrofuran / 96 h / 20 °C

With dmap; sodium hydroxide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1016/j.bmc.2004.11.053