2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

Base Information

Chemical Name:2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate
CAS No.:478316-17-5
Molecular Formula:C₂₀H₂₅N₃O₃S
Molecular Weight:387.503
Hs Code.:

Synonyms:2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

Chemical Property:

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Technology Process of 2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

There total 3 articles about 2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 143-33-9,25596-52-5
sodium cyanide

: 506-59-2
N,N-dimethylammonium chloride

: 478316-14-2
5-(N,N-diethylamino)-2-formylphenyl benzenesulfonate

: 478316-17-5
2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

Guidance literature:: In water; acetonitrile; at 20 ℃;
DOI:10.1021/jo025767j

Reference yield:

: 17754-90-4
4-(Diethylamino)salicylaldehyde

: 478316-17-5
2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / K₂CO₃ / acetone / 2 h / 20 °C

2: 84 percent / H₂O; acetonitrile / 20 °C

With potassium carbonate; In water; acetone; acetonitrile;
DOI:10.1021/jo025767j

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 478316-17-5
2-(cyano-N,N-dimethylamino)methyl-5-N,N-diethylaminophenyl benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / K₂CO₃ / acetone / 2 h / 20 °C

2: 84 percent / H₂O; acetonitrile / 20 °C

With potassium carbonate; In water; acetone; acetonitrile;
DOI:10.1021/jo025767j