bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

Base Information

Chemical Name:bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate
CAS No.:1019648-68-0
Molecular Formula:C₂₂H₁₉Cl₆N₃O₆
Molecular Weight:634.127
Hs Code.:

Synonyms:bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

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Chemical Property of bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

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Technology Process of bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

There total 7 articles about bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₇N₃O₂

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1019648-68-0
bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.166667h;

Reference yield:

: 24393-56-4,51507-22-3,1929-30-2
ethyl p-methoxycinnamate

: 1019648-68-0
bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 0 - 35 °C

2.1: ammonium formate / palladium 10% on activated carbon / ethanol / 3 h / Reflux

2.2: 3 h / 120 °C

3.1: potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

With potassium phosphate; copper(l) iodide; ammonium formate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N,N`-dimethylethylenediamine; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; ethanol;

Reference yield:

: 745060-01-9
ethyl 3-(4-methoxyphenyl)-4-nitrobutanoate

: 1019648-68-0
bis(2,2,2-trichloroethyl)(4-(4-(4-methoxyphenyl)-2-oxopyrrolidin-1-yl)pyridin-2-yl)imidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium formate / palladium 10% on activated carbon / ethanol / 3 h / Reflux

1.2: 3 h / 120 °C

2.1: potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

With potassium phosphate; copper(l) iodide; ammonium formate; triethylamine; N,N`-dimethylethylenediamine; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; ethanol;