(4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

Base Information

• Chemical Name: (4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one
• CAS No.: 1067232-65-8
• Molecular Formula: C₁₈H₂₅NO₄
• Molecular Weight: 319.401

Synonyms:(4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

Chemical Property of (4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

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Technology Process of (4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

There total 1 articles about (4S,1'R,2'S)-N⁽³⁾-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

methanol (67-56-1) + (S)-N(3)-(cyclohexyl-1'-en-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-64-7) → (4S,1'S,2'R)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-66-9) + (4S,1'S,2'S)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-67-0) + (4S,1'R,2'R)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one + (4S,1'R,2'S)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-65-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In methanol; at -20 ℃; for 4h;

DOI:10.1016/j.tet.2008.07.012

Reference yield: 55.0%

(4S,1'R,2'S)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-65-8) → cyclohexanone-2-ol (533-60-8)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.tet.2008.07.012

Reference yield: 9.0%

(4S,1'R,2'S)-N(3)-(1'-methoxy-2'-hydroxy-cyclohex-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-65-8) + benzyl bromide (100-39-0) → (S)-2-(benzyloxy)cyclohexan-1-one (153381-46-5)

Guidance literature:

With sodium hydride; In chloroform-d1; at 20 ℃; for 10h;

DOI:10.1016/j.tet.2008.07.012

upstream raw materials:

methanol

(S)-N⁽³⁾-(cyclohexyl-1'-en-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

Downstream raw materials:

cyclohexanone-2-ol

(S)-2-(benzyloxy)cyclohexan-1-one

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