1-phenyl-2-nitroethyl methyl ether

Base Information

• Chemical Name: 1-phenyl-2-nitroethyl methyl ether
• CAS No.: 3532-58-9
• Molecular Formula: C₉H₁₁NO₃
• Molecular Weight: 181.191

Synonyms:1-phenyl-2-nitroethyl methyl ether

Chemical Property of 1-phenyl-2-nitroethyl methyl ether

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 1-phenyl-2-nitroethyl methyl ether

There total 5 articles about 1-phenyl-2-nitroethyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

methanol (67-56-1) + (2-nitroethenyl)benzene (102-96-5) → 1-phenyl-2-nitroethyl methyl ether (3532-58-9)

Guidance literature:

With nickel(II) ferrite; at 80 ℃; for 2h; Green chemistry;

DOI:10.1039/c6ra21160g

Reference yield: 60.0%

nitrostyrene (5153-67-3) + sodium methylate (124-41-4) → 1-phenyl-2-nitroethyl methyl ether (3532-58-9)

Guidance literature:

In methanol; Ambient temperature;

DOI:10.1016/0223-5234(96)88314-0

Reference yield: 37.0%

(2-nitroethenyl)benzene (102-96-5) + sodium methylate (124-41-4) → 1-phenyl-2-nitroethyl methyl ether (3532-58-9)

Guidance literature:

In methanol; at 20 ℃; for 0.25h; Reagent/catalyst; Inert atmosphere;

DOI:10.1016/j.tet.2014.10.042

upstream raw materials:

methanol

(2-nitroethenyl)benzene

2-nitro-1-nitrosoethylbenzene

sodium methylate

Downstream raw materials:

2-methoxy-2-phenylethan-1-amine

N-(β-methoxy-phenethyl)-phthalamic acid methyl ester

N-(β-methoxy-phenethyl)-phthalamic acid

2-[(E)-2-phenylvinyl]-1H-isoindole-1,3(2H)-dione

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