3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

Base Information

Chemical Name:3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride
CAS No.:119843-52-6
Molecular Formula:C₁₇H₁₁ClF₂N₄O
Molecular Weight:360.75
Hs Code.:

Synonyms:3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

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Technology Process of 3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

There total 6 articles about 3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-37-8
oxalyl dichloride

: 118875-13-1
3,3-bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoic acid

: 119843-52-6
3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

Guidance literature:: In dichloromethane;

Reference yield:

: 118875-13-1
3,3-bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoic acid

: 119843-52-6
3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane;
DOI:10.1021/jm00129a004

Reference yield:

: 118875-18-6
ethyl 2-cyano-3,3-bis(4-fluorophenyl)-2-propenoate

: 119843-52-6
3,3-Bis(4-fluorophenyl)-2-(1-methyl-1H-tetrazol-5-yl)-2-propenoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: tri-n-butyltin azide / 110 - 120 °C

2: 52 percent / NaH / tetrahydrofuran

3: aq. LiOH

4: oxalyl chloride / CH₂Cl₂

With lithium hydroxide; oxalyl dichloride; tri-n-butyltin azide; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00129a004