dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

Base Information

Chemical Name:dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester
CAS No.:877465-02-6
Molecular Formula:C₅₇H₅₈S₂
Molecular Weight:807.22
Hs Code.:

dithioformic acid 4-<i>tert</i>-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

Synonyms:dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

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Chemical Property of dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

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Technology Process of dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

There total 1 articles about dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 75-15-0,12122-00-8
carbon disulfide

: 177971-43-6
(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

: 877465-02-6
dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

Guidance literature:: (4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br; With tert.-butyl lithium; at -78 ℃;

carbon disulfide; at -78 ℃;
DOI:10.1246/cl.2005.1674

Reference yield: 79.0%

: 877465-02-6
dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

: 74-88-4
methyl iodide

: C₅₉H₆₂S₂

: C₁₁₆H₁₂₀S₄

Guidance literature:: dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; at -98 ℃; for 0.0833333h;

methyl iodide; In tetrahydrofuran; at -98 ℃;
DOI:10.1246/cl.2005.1674

Reference yield: 74.0%

: 877465-02-6
dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

: 74-88-4
methyl iodide

: C₅₇H₆₀S

Guidance literature:: dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; at -30 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at -30 ℃;
DOI:10.1246/cl.2005.1674