(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

Base Information

Chemical Name:(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt
CAS No.:1335202-22-6
Molecular Formula:C₂H₂O₄*C₂₀H₂₅ClN₆O
Molecular Weight:490.947
Hs Code.:

Synonyms:(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

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Chemical Property of (2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

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Technology Process of (2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

There total 1 articles about (2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335202-21-5
(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol

: 144-62-7,97993-78-7
oxalic acid

: 1335202-22-6
(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

Guidance literature:: In tetrahydrofuran; at 45 ℃; for 0.25h;

Reference yield:

: 1335202-22-6
(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

: 1335202-21-5
(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol

Guidance literature:: With sodium hydroxide; In dichloromethane; water; for 0.333333h;

Reference yield:

: 1335202-22-6
(2R)-2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol oxalate salt

: 1335202-19-1
(2R)-2-[8-(2-Chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]propan-1-ol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / dichloromethane; water / 0.33 h

2: hydrogenchloride / 1,4-dioxane; diethyl ether / 2.5 h / 20 °C

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane; diethyl ether; dichloromethane; water;