1,2-Dimethoxy-4-[(4-methoxyphenyl)methyl]benzene

Base Information

• Chemical Name: 1,2-Dimethoxy-4-[(4-methoxyphenyl)methyl]benzene
• CAS No.: 2898-55-7
• Molecular Formula: C₁₆H₁₈O₃
• Molecular Weight: 258.317
• DSSTox Substance ID: DTXSID001240516
• Nikkaji Number: J2.166.551G

Synonyms:1,2-dimethoxy-4-[(4-methoxyphenyl)methyl]benzene;2898-55-7;DTXSID001240516

Chemical Property of 1,2-Dimethoxy-4-[(4-methoxyphenyl)methyl]benzene

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 258.125594432
• Heavy Atom Count: 19
• Complexity: 248

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)CC2=CC(=C(C=C2)OC)OC

Technology Process of 1,2-Dimethoxy-4-[(4-methoxyphenyl)methyl]benzene

There total 10 articles about 1,2-Dimethoxy-4-[(4-methoxyphenyl)methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

bis[(p-anisyl)(3,4-dimethoxyphenyl)methyl] ether (1426391-14-1) → 3,4,4'-trimethoxybenzophenone (2898-54-6) + (3,4-dimethoxy-phenyl)-(4-methoxy-phenyl)-methane (2898-55-7)

Guidance literature:

With iodine; In neat (no solvent); at 85 ℃; for 0.25h;

DOI:10.1039/c3ob27267b

Reference yield:

1,2-dimethoxybenzene (91-16-7) + p-methoxybenzyl acetate (104-21-2) → (3,4-dimethoxy-phenyl)-(4-methoxy-phenyl)-methane (2898-55-7)

Guidance literature:

With trifluorormethanesulfonic acid; at 20 ℃; for 1h; Neat (no solvent);

DOI:10.1016/j.tetlet.2011.01.033

Reference yield:

veratryl acetate (53751-40-9) + methoxybenzene (100-66-3) → (3,4-dimethoxy-phenyl)-(4-methoxy-phenyl)-methane (2898-55-7)

Guidance literature:

With trifluorormethanesulfonic acid; at 20 ℃; for 0.333333h; Neat (no solvent);

DOI:10.1016/j.tetlet.2011.01.033

upstream raw materials:

3,4,4'-trimethoxybenzophenone

4-hydroxy-3,4'-dimethoxy-benzophenone

1,2-dimethoxy-4-methylbenzene

methoxybenzene

Downstream raw materials:

3,4,4'-trimethoxybenzophenone

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