1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

Base Information

Chemical Name:1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane
CAS No.:1022983-26-1
Molecular Formula:C₂₅H₃₁N₅O₂S
Molecular Weight:465.619
Hs Code.:

Synonyms:1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

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Chemical Property of 1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

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Technology Process of 1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

There total 1 articles about 1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6959-47-3
2-chloromethylpyridine hydrochloride

: 129422-96-4
1-(p-toluenesulfonyl)-1,4,7-triazacyclononane

: 1022983-26-1
1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

Guidance literature:: With tetrabutylammomium bromide; sodium carbonate; In acetonitrile; for 22h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201303317

Reference yield: 80.65%

: 1022983-26-1
1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

: 75-09-2
dichloromethane

: Ni⁽²⁺⁾*2CF₃O₃S^(1-)*2C₂H₃N

: C₂₆H₃₁F₃N₅NiO₅S₂⁽¹⁺⁾*CF₃O₃S^(1-)*0.5CH₂Cl₂

Guidance literature:: 1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane; Ni⁽²⁺⁾*2CF₃O₃S^(1-)*2C₂H₃N; In tetrahydrofuran; for 4h; Inert atmosphere; Glovebox;

dichloromethane; Inert atmosphere; Glovebox;
DOI:10.1002/chem.201303317

Reference yield: 76.9%

: 1022983-26-1
1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane

: iron(II) trifluoromethanesulfonate acetonitrile disolvate

: 75-09-2
dichloromethane

: C₂₆H₃₁F₃FeN₅O₅S₂⁽¹⁺⁾*CF₃O₃S^(1-)*0.5CH₂Cl₂

Guidance literature:: 1-(p-toluenesulfonyl)-4,7-di(picolyl)-1,4,7-triazacyclononane; iron(II) trifluoromethanesulfonate acetonitrile disolvate; In tetrahydrofuran; for 5h; Inert atmosphere; Glovebox;

dichloromethane; Inert atmosphere; Glovebox;
DOI:10.1002/chem.201303317