Technology Process of C26H21N
There total 3 articles about C26H21N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(1,5-cyclooctadiene)nickel(0); potassium tert-butylate; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate;
In
tetrahydrofuran; toluene; butan-1-ol;
at 20 ℃;
for 24h;
enantiospecific reaction;
Inert atmosphere;
DOI:10.1021/ja311783k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
2.1: bis(1,5-cyclooctadiene)nickel(0); N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere
With
bis(1,5-cyclooctadiene)nickel(0); potassium tert-butylate; sodium hydride; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene; butan-1-ol;
DOI:10.1021/ja311783k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Inert atmosphere
2: bis(1,5-cyclooctadiene)nickel(0); N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere
With
bis(1,5-cyclooctadiene)nickel(0); potassium tert-butylate; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate;
In
tetrahydrofuran; toluene; butan-1-ol;
DOI:10.1021/ja311783k
