(2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

Base Information

Chemical Name:(2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate
CAS No.:1201554-52-0
Molecular Formula:C₂₆H₃₉NO₄Si
Molecular Weight:457.685
Hs Code.:

Synonyms:(2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

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Technology Process of (2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

There total 1 articles about (2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1201554-50-8
(2R,3S)-tert-butyl 2-hydroxy-3-(4-methoxyphenylamino)-3-phenylpropanoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1201554-52-0
(2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jo101559p

Reference yield:

: 1201554-52-0
(2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate

: 98-88-4
benzoyl chloride

: 1201554-54-2
C₂₆H₃₇NO₄Si

Guidance literature:: (2R,3S)-tert-butyl 2-(tert-butyldimethylsilyloxy)-3-(4-methoxyphenylamino)-3-phenylpropanoate; With ammonium cerium (IV) nitrate; In acetonitrile; at 0 ℃; for 1h;

With triethylamine; In dichloromethane; at 20 ℃; for 0.25h;

benzoyl chloride; Further stages;
DOI:10.1039/c9ob02149c