9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

Base Information

Chemical Name:9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine
CAS No.:171075-64-2
Molecular Formula:C₃₂H₃₃N₅O₆S
Molecular Weight:615.71
Hs Code.:

9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N<sup>6</sup>,N<sup>6</sup>-dimethyladenine

Synonyms:9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

Suppliers and Price of 9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

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Technology Process of 9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

There total 1 articles about 9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 124-40-3
dimethyl amine

: 156420-36-9
6-chloro-9-(2-O-acetyl-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)purine

: 171075-64-2
9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

Guidance literature:: In water; N,N-dimethyl-formamide; at 4 ℃;
DOI:10.1248/cpb.43.955

Reference yield: 21.0%

: 171075-64-2
9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

: 171075-66-4
9-(3-azido-3-deoxy-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

: 171075-65-3
9-(2-azido-2-deoxy-5-O-trityl-β-D-xylofuranosyl)-N⁶,N⁶-dimethyladenine

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; for 1h;
DOI:10.1248/cpb.43.955

Reference yield:

: 171075-64-2
9-(3-O-methanesulfonyl-5-O-trityl-β-D-arabinofuranosyl)-N⁶,N⁶-dimethyladenine

: 171075-68-6
9-(3-amino-2-fluoro-2,3-dideoxy-5-O-trityl-β-D-ribofuranosyl)-N⁶,N⁶-dimethyladenine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaN₃ / dimethylformamide / 1 h / 100 °C

2: 72 percent / DAST, pyridine / CH₂Cl₂ / 6 h / 50 °C

3: 90 percent / H₂ / Pd-C / ethanol; acetic acid / 3 h / Ambient temperature

With pyridine; sodium azide; hydrogen; 4,4'-diaminostilbene-2,2'-disulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.43.955