L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

Base Information

Chemical Name:L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt
CAS No.:104849-11-8
Molecular Formula:C₂H₄O₂*C₂₉H₄₄N₄O₇
Molecular Weight:620.744
Hs Code.:

Synonyms:L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

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Chemical Property of L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

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Technology Process of L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

There total 3 articles about L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 104849-09-4
N-(benzyloxycarbonyl)-L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline

: 64-19-7,77671-22-8
acetic acid

: 104849-11-8
L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h;
DOI:10.1021/jm00384a013

Reference yield:

: 104849-08-3
N-(benzyloxycarbonyl)-L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline methyl ester

: 104849-11-8
L-phenylalanyl-D-alanyl-L-2-amino-7-(tert-butyloxycarbonyl)heptanoyl-D-proline acetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1.0 N aq. NaOH / methanol / Ambient temperature

2: 83 percent / H₂ / 10percent Pd/C / methanol / 3 h

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00384a013