4-trifluoromethylbenzyl methanesulfonate

Base Information

• Chemical Name: 4-trifluoromethylbenzyl methanesulfonate
• CAS No.: 96258-56-9
• Molecular Formula: C₉H₉F₃O₃S
• Molecular Weight: 254.23

Synonyms:4-trifluoromethylbenzyl methanesulfonate

Chemical Property of 4-trifluoromethylbenzyl methanesulfonate

Chemical Property:

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Technology Process of 4-trifluoromethylbenzyl methanesulfonate

There total 1 articles about 4-trifluoromethylbenzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

4-(trifluoromethyl)benzylic alcohol (349-95-1) + methanesulfonyl chloride (124-63-0) → 4-trifluoromethylbenzyl methanesulfonate (96258-56-9)

Guidance literature:

With triethylamine; In dichloromethane; at -50 ℃; for 0.5h;

DOI:10.5935/0103-5053.20130121

Reference yield: 100.0%

1-hydroxy-naphthalene-2-carboxylic acid methyl ester (948-03-8) + 4-trifluoromethylbenzyl methanesulfonate (96258-56-9) → methyl 1-[[4-(trifluoromethyl)phenyl]methoxy]naphthalene-2-carboxylate (1000386-58-2)

Guidance literature:

With potassium carbonate; In acetone; at 50 ℃;

Reference yield: 81.0%

4-trifluoromethylbenzyl methanesulfonate (96258-56-9) → 1-(azidomethyl)-4-(trifluoromethyl)benzene (222716-19-0)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 20 ℃; for 15h;

DOI:10.5935/0103-5053.20130121

upstream raw materials:

4-(trifluoromethyl)benzylic alcohol

methanesulfonyl chloride

Downstream raw materials:

1-(4-trifluoromethylbenzyl)indole-4-carbaldehyde

1-(azidomethyl)-4-(trifluoromethyl)benzene

methyl 1-[[4-(trifluoromethyl)phenyl]methoxy]naphthalene-2-carboxylate

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