3-acetylphenyl methanesulfonate

Base Information

Chemical Name:3-acetylphenyl methanesulfonate
CAS No.:1092513-16-0
Molecular Formula:C₉H₁₀O₄S
Molecular Weight:214.242
Hs Code.:

Synonyms:3-acetylphenyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-acetylphenyl methanesulfonate

Chemical Property:

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Technology Process of 3-acetylphenyl methanesulfonate

There total 1 articles about 3-acetylphenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 121-71-1
3-Hydroxyacetophenone

: 124-63-0
methanesulfonyl chloride

: 1092513-16-0
3-acetylphenyl methanesulfonate

Guidance literature:: With triethylamine; In ethyl acetate; at 0 - 20 ℃; for 0.166667h; Green chemistry;
DOI:10.1055/s-0034-1378867

Reference yield: 95.0%

: 1092513-16-0
3-acetylphenyl methanesulfonate

: 1423-26-3
(meta-(trifluoromethyl)phenyl)boronic acid

: 352032-25-8
1-(3'-(trifluoromethyl)biphenyl-3-yl)ethanone

Guidance literature:: With potassium phosphate; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; palladium diacetate; In tert-Amyl alcohol; at 20 - 110 ℃; Inert atmosphere;
DOI:10.1021/ol9015892

Reference yield: 94.0%

: 1092513-16-0
3-acetylphenyl methanesulfonate

: 32316-92-0
naphthalene-2-boronic acid

: 1067883-71-9
3'-(2-naphthyl)acetophenone

Guidance literature:: With potassium phosphate; C₅₈H₇₂N₂O₄P₂Pd₂; In tert-butyl alcohol; at 110 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.200803193