(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Base Information

Chemical Name:(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene
CAS No.:84056-97-3
Molecular Formula:C₃₅H₅₀O₂S
Molecular Weight:534.847
Hs Code.:

(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Synonyms:(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Suppliers and Price of (3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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Chemical Property of (3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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Technology Process of (3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

There total 8 articles about (3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67-56-1
methanol

: 84051-53-6
(E)-2-((3S,8S,9S,10R,13S,14S,17S)-3-Methoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-6-methyl-5-phenylsulfanyl-hepta-3,5-dien-2-ol

: 84056-97-3
(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Guidance literature:: With nickel dichloride;
DOI:10.1021/ja00341a051

Reference yield: 84.0%

: 67-56-1
methanol

: 84051-53-6
(E)-2-((3S,8S,9S,10R,13S,14S,17S)-3-Methoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-6-methyl-5-phenylsulfanyl-hepta-3,5-dien-2-ol

: 84056-97-3
3β,25-dimethoxy-24-(phenylthio)-cholesta-5,20(22),23-triene

Guidance literature:: With nickel dichloride; for 2h; Heating;
DOI:10.1021/jo00180a025

Reference yield:

: 511-26-2
pregnenolone methyl ether

: 84056-97-3
(3S,8S,9S,10R,13S,14S,17R)-3-Methoxy-17-((1Z,3Z)-5-methoxy-1,5-dimethyl-4-phenylsulfanyl-hexa-1,3-dienyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / 1.) sec-BuLi / 1.) THF-HMPA, -78 deg C

2: 39 percent / sec-BuLi / 1.) HMPA-THF, -78 deg C, 1 h, 2.) 0 deg C

3: 84 percent / NiCl₂

With sec.-butyllithium; nickel dichloride;
DOI:10.1021/ja00341a051