2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide

Base Information

• Chemical Name: 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide
• CAS No.: 103076-38-6
• Molecular Formula: C₁₅H₂₁ClN₂OS₂
• Molecular Weight: 344.93

Synonyms:2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide

Chemical Property of 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide

Chemical Property:

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Technology Process of 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide

There total 2 articles about 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

2-(4-chlorobutoxy)benzaldehyde (114258-52-5) + methyl thioisocyanate (556-61-6) + Cysteamine (60-23-1) → 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide (103076-38-6)

Guidance literature:

DOI:10.1248/cpb.35.2394

Reference yield:

salicylaldehyde (90-02-8) → 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide (103076-38-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 68 h / Ambient temperature

2: 47 percent

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.35.2394

Reference yield: 40.0%

4-phenyl-1-piperazine (92-54-6) + 2-[2-(4-Chloro-butoxy)-phenyl]-thiazolidine-3-carbothioic acid methylamide (103076-38-6) → 2-{2-[4-(4-Phenyl-piperazin-1-yl)-butoxy]-phenyl}-thiazolidine-3-carbothioic acid methylamide (103073-26-3)

Guidance literature:

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 20h;

DOI:10.1248/cpb.35.2394

upstream raw materials:

2-(4-chlorobutoxy)benzaldehyde

methyl thioisocyanate

Cysteamine

salicylaldehyde

Downstream raw materials:

2-{2-[4-(4-Phenyl-piperazin-1-yl)-butoxy]-phenyl}-thiazolidine-3-carbothioic acid methylamide

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