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C28H26Cl3FO7S2

Base Information
  • Chemical Name:C28H26Cl3FO7S2
  • CAS No.:1055304-23-8
  • Molecular Formula:C28H26Cl3FO7S2
  • Molecular Weight:664
  • Hs Code.:
C<sub>28</sub>H<sub>26</sub>Cl<sub>3</sub>FO<sub>7</sub>S<sub>2</sub>

Synonyms:C28H26Cl3FO7S2

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Chemical Property of C28H26Cl3FO7S2
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Technology Process of C28H26Cl3FO7S2

There total 10 articles about C28H26Cl3FO7S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;
Guidance literature:
Multi-step reaction with 2 steps
1: lithium hydroxide; water / 1,4-dioxane / 0.25 h / 20 °C
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C
With dmap; lithium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;
Guidance literature:
Multi-step reaction with 5 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 0 °C
1.2: 18 h / 0 °C
2.1: sodium hydroxide; water / tetrahydrofuran / 29 h / 0 - 20 °C
2.2: pH 2
3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C
4.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C
5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C
With dmap; sodium hydroxide; boron trifluoride diethyl etherate; water; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
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