Technology Process of C32H43N3O5
There total 16 articles about C32H43N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 1) NaOEt, 2) aq. KOH / 1) EtOH
2: dimethylformamide / Heating
3: TsOH / toluene
4: NaNO2, CF3CO2H
5: aq. KOH
6: SOCl2 / Heating
7: SnCl4 / CH2Cl2; nitromethane / Ambient temperature
8: B2H6 / tetrahydrofuran
9: H2, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr
10: PhCH2ONa / 100 °C / 12 Torr
11: H2 / 10percent Pd/C / tetrahydrofuran / 760 Torr
With
potassium hydroxide; thionyl chloride; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
under 760 Torr;
- Guidance literature:
-
Multi-step reaction with 12 steps
1: HBr
2: 1) NaOEt, 2) aq. KOH / 1) EtOH
3: dimethylformamide / Heating
4: TsOH / toluene
5: NaNO2, CF3CO2H
6: aq. KOH
7: SOCl2 / Heating
8: SnCl4 / CH2Cl2; nitromethane / Ambient temperature
9: B2H6 / tetrahydrofuran
10: H2, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr
11: PhCH2ONa / 100 °C / 12 Torr
12: H2 / 10percent Pd/C / tetrahydrofuran / 760 Torr
With
potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; sodium ethanolate; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;