3-ethyl-4-methoxybenzene boronic acid

Base Information

• Chemical Name: 3-ethyl-4-methoxybenzene boronic acid
• CAS No.: 947547-41-3
• Molecular Formula: C₉H₁₃BO₃
• Molecular Weight: 180.011
• Mol file: 947547-41-3.mol

Synonyms:3-ethyl-4-methoxybenzene boronic acid

Chemical Property of 3-ethyl-4-methoxybenzene boronic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-Ethyl-4-methoxyphenylboronicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-ethyl-4-methoxybenzene boronic acid

There total 1 articles about 3-ethyl-4-methoxybenzene boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

4-bromo-2-ethyl-1-methoxybenzene (33839-11-1) → 3-ethyl-4-methoxybenzene boronic acid (947547-41-3)

Guidance literature:

4-bromo-2-ethyl-1-methoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; hexane; water;

Reference yield: 65.0%

3-ethyl-4-methoxybenzene boronic acid (947547-41-3) + 5-Bromo-1-indanone (34598-49-7) → 5-(3-ethyl-4-methoxyphenyl)indan-1-one (947547-42-4)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 24h; Heating / reflux;

Reference yield: 60.0%

4-(4-bromophenyl)-2,2-dimethyl-4-oxo-butyric acid (791593-72-1) + 3-ethyl-4-methoxybenzene boronic acid (947547-41-3) → 4-(3'-ethyl-4'-methoxy-biphenyl-4-yl)-2,2-dimethyl-4-oxo-butyric acid (947547-98-0)

Guidance literature:

4-(4-bromophenyl)-2,2-dimethyl-4-oxo-butyric acid; 3-ethyl-4-methoxybenzene boronic acid; With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 19h; Heating / reflux;

With water; In ethanol; toluene;

upstream raw materials:

4-bromo-2-ethyl-1-methoxybenzene

Downstream raw materials:

5-(3-ethyl-4-methoxyphenyl)indan-1-one

4-(3'-ethyl-4'-methoxy-biphenyl-4-yl)-2,2-dimethyl-4-oxo-butyric acid

[5-(3-ethyl-4-methoxyphenyl)-2-thienyl](3-hydroxyphenyl)methanone