3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

Base Information

Chemical Name:3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester
CAS No.:105916-78-7
Molecular Formula:C₃₄H₃₂N₄O₅
Molecular Weight:576.652
Hs Code.:

3-(4-<i>tert</i>-butoxy-phenyl)-2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

Synonyms:3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

Chemical Property:

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Technology Process of 3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

There total 2 articles about 3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71989-38-3,118488-18-9,204384-67-8
Fmoc-Tyr(tBu)-OH

: 2592-95-2
benzotriazol-1-ol

: 105916-78-7
3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1021/ol035774+

Reference yield:

: 105916-78-7
3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

Guidance literature:

Reference yield: 51.0%

: C₂₉H₃₀NO₅Pol

: 117830-91-8
C₂₇H₂₅N₅O₅S

: 127633-31-2
Fmoc-Phe-benzotriazolyl ester

: 124007-49-4
Fmoc-Glu(t-Bu)-benzotriazolyl ester

: 105916-79-8
(S)-3-tert-Butoxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

: 117830-89-4
Fmoc-Gly-OBt

: 105916-78-7
3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester

: 1191395-91-1
H-Glu-Tyr-Gly-Ser-Phe-Phe-Cys(Acm)-Glu-Leu-OH

Guidance literature:: C₂₉H₃₀NO₅Pol; With piperidine; In 1-methyl-pyrrolidin-2-one; for 0.333333h; Automated synthesizer; solid phase reaction;

Fmoc-Glu(t-Bu)-benzotriazolyl ester; In 1-methyl-pyrrolidin-2-one; for 1.16667h; Automated synthesizer; solid phase reaction;

C₂₇H₂₅N₅O₅S; Fmoc-Phe-benzotriazolyl ester; (S)-3-tert-Butoxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester; Fmoc-Gly-OBt; 3-(4-tert-butoxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid benzotriazol-1-yl ester; Further stages;
DOI:10.1134/S1068162009030029