1-O-trimethylsilyloxy-3-hexanthiol

Base Information

• Chemical Name: 1-O-trimethylsilyloxy-3-hexanthiol
• CAS No.: 1251531-33-5
• Molecular Formula: C₉H₂₂OSSi
• Molecular Weight: 206.425
• Mol file: 1251531-33-5.mol

Synonyms:1-O-trimethylsilyloxy-3-hexanthiol

Chemical Property of 1-O-trimethylsilyloxy-3-hexanthiol

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-O-trimethylsilyloxy-3-hexanthiol

There total 1 articles about 1-O-trimethylsilyloxy-3-hexanthiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + 3-mercapto-1-hexanol (90180-88-4,90180-90-8,51755-83-0) → 1-O-trimethylsilyloxy-3-hexanthiol (1251531-33-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jf102022s

Reference yield:

1-O-trimethylsilyloxy-3-hexanthiol (1251531-33-5) → 3,3'-disulfanediyldihexan-1-ol (344738-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: 2.27 h / 60 - 100 °C / 1 - 9 Torr / Pyrolysis

With pyridine;

DOI:10.1021/jf102022s

upstream raw materials:

chloro-trimethyl-silane

3-mercapto-1-hexanol

Downstream raw materials:

3,3'-disulfanediyldihexan-1-ol

Refernces