methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

Base Information

Chemical Name:methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate
CAS No.:388566-87-8
Molecular Formula:C₂₀H₂₂O₇
Molecular Weight:374.39
Hs Code.:

Synonyms:methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

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Technology Process of methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

There total 3 articles about methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67-56-1
methanol

: 388566-86-7
(E)-3-(3’-hydroxy-4’-methoxyphenyl)-2-(3”,4”,5”-trimethoxyphenyl)-2-propenoic acid

: 388566-87-8
methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

Guidance literature:: With sulfuric acid; Heating;
DOI:10.1021/jo015959z

Reference yield:

: 621-59-0
isovanillin

: 388566-87-8
methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine / acetic anhydride / 3 h / Heating

2: 80 percent / conc. H₂SO₄ / Heating

With sulfuric acid; triethylamine; In acetic anhydride; 1: Perkin condensation;
DOI:10.1021/jo015959z

Reference yield:

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 388566-87-8
methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine / acetic anhydride / 3 h / Heating

2: 80 percent / conc. H₂SO₄ / Heating

With sulfuric acid; triethylamine; In acetic anhydride; 1: Perkin condensation;
DOI:10.1021/jo015959z