4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

Base Information

Chemical Name:4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide
CAS No.:1093988-02-3
Molecular Formula:C₂₅H₂₃BrCl₂FN₃O₅S
Molecular Weight:647.349
Hs Code.:

Synonyms:4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

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Chemical Property of 4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

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Technology Process of 4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

There total 9 articles about 4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874974-99-9
2-{3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetohydrazide

: 1213-06-5
Antidipsin

: 1093988-02-3
4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 33863-76-2
1-bromo-3-chloro-5-fluorobenzene

: 1093988-02-3
4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,N-dimethyl-formamide / 20 °C

2.1: boron tribromide / dichloromethane / 20 °C

2.2: 20 °C

3.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

4.2: 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 60 °C

5.2: 0 °C

6.1: sodium dithionite / tetrahydrofuran; water / 1 h / 20 °C

7.1: tert.-butylnitrite; copper dichloride / acetonitrile / 0.25 h / 50 °C

8.1: hydrazine / ethanol / 8 h / Reflux

9.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With tert.-butylnitrite; sodium dithionite; boron tribromide; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; copper dichloride; sodium t-butanolate; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 174913-12-3
1-bromo-3-chloro-5-methoxybenzene

: 1093988-02-3
4-{[2-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)hydrazino]carbonyl}-N,N-diethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron tribromide / dichloromethane / 20 °C

1.2: 20 °C

2.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 60 °C

4.2: 0 °C

5.1: sodium dithionite / tetrahydrofuran; water / 1 h / 20 °C

6.1: tert.-butylnitrite; copper dichloride / acetonitrile / 0.25 h / 50 °C

7.1: hydrazine / ethanol / 8 h / Reflux

8.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With tert.-butylnitrite; sodium dithionite; boron tribromide; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; copper dichloride; sodium t-butanolate; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;