(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

Base Information

Chemical Name:(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane
CAS No.:784178-01-4
Molecular Formula:C₂₆H₃₉N₃O₅S₂
Molecular Weight:537.745
Hs Code.:

Synonyms:(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

Suppliers and Price of (2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

There total 1 articles about (2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-24-7
acetic anhydride

: 131078-72-3
4-methyl-N-((1S)-2-methyl-1-{[((2S)-3-methyl-2-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]methyl}propyl)benzenesulfonamide

: 784178-01-4
(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

Guidance literature:: for 4h; Heating;
DOI:10.1039/b409259g

Reference yield: 74.0%

: 784178-01-4
(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

: 6315-52-2
1,2-bis-tosyloxyethane

: 784178-04-7
(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: With caesium carbonate; In acetonitrile; for 144h; Heating;
DOI:10.1039/b409259g

Reference yield:

: 784178-01-4
(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

: 784178-07-0
(2S,6S)-2,6-di(1-methylethyl)-4-ethyl-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Cs₂CO₃ / acetonitrile / 144 h / Heating

2: 51 percent / LiAlH₄ / tetrahydrofuran / 18 h / Heating

With lithium aluminium tetrahydride; caesium carbonate; In tetrahydrofuran; acetonitrile; 1: Richman-Atkins reaction;
DOI:10.1039/b409259g