(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Base Information

Chemical Name:(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane
CAS No.:784178-04-7
Molecular Formula:C₂₈H₄₁N₃O₅S₂
Molecular Weight:563.783
Hs Code.:

Synonyms:(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

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Technology Process of (2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

There total 2 articles about (2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 784178-01-4
(2S,6S)-4-acetyl-1,7-di-p-toluenesulfonyl-2,6-di(1-methylethyl)-1,4,7-triazaheptane

: 6315-52-2
1,2-bis-tosyloxyethane

: 784178-04-7
(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: With caesium carbonate; In acetonitrile; for 144h; Heating;
DOI:10.1039/b409259g

Reference yield:

: 131078-72-3
4-methyl-N-((1S)-2-methyl-1-{[((2S)-3-methyl-2-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]methyl}propyl)benzenesulfonamide

: 784178-04-7
(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 4 h / Heating

2: 74 percent / Cs₂CO₃ / acetonitrile / 144 h / Heating

With caesium carbonate; In acetonitrile; 2: Richman-Atkins reaction;
DOI:10.1039/b409259g