(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Base Information

Chemical Name:(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane
CAS No.:417699-65-1
Molecular Formula:C₂₆H₃₉N₃O₄S₂
Molecular Weight:521.745
Hs Code.:

Synonyms:(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Suppliers and Price of (2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

There total 8 articles about (2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 784178-04-7
(2S,6S)-4-acetyl-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

: 417699-65-1
(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: With hydrogenchloride; In ethanol; for 96h; Heating;
DOI:10.1039/b409259g

Reference yield:

: (3S,8S)-3,8-Diisopropyl-4,7-bis-(toluene-4-sulfonyl)-[1,4,7]triazonane-1-carboxylic acid benzyl ester

: 417699-65-1
(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 3h;
DOI:10.1021/ol025513k

Reference yield:

: 131078-72-3
4-methyl-N-((1S)-2-methyl-1-{[((2S)-3-methyl-2-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]methyl}propyl)benzenesulfonamide

: 417699-65-1
(2S,6S)-2,6-di(1-methylethyl)-1,7-di-p-toluenesulfonyl-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 4 h / Heating

2: 74 percent / Cs₂CO₃ / acetonitrile / 144 h / Heating

3: 63 percent / aq. HCl / ethanol / 96 h / Heating

With hydrogenchloride; caesium carbonate; In ethanol; acetonitrile; 2: Richman-Atkins reaction;
DOI:10.1039/b409259g