N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

Base Information

Chemical Name:N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid
CAS No.:449779-67-3
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

Synonyms:N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

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Chemical Property of N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

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Technology Process of N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

There total 4 articles about N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 75-36-5
acetyl chloride

: 279215-16-6
2,4-dihydroxy-3,5-dipropylbenzoic acid

: 449779-67-3
N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

Guidance literature:: acetyl chloride; 2,4-dihydroxy-3,5-dipropylbenzoic acid; With pyridine; In dichloromethane; at 0 - 25 ℃; for 1h;

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 1h; Heating;

N-methylhydroxyamine hydrochloride; With sodium carbonate; In diethyl ether; dichloromethane; for 0.5h;
DOI:10.1021/jm0502135

Reference yield:

: 860780-50-3
methyl 2,4-bis(allyloxy)benzoate

: 449779-67-3
N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 81 percent / various solvent(s) / 7 h / Heating

2.1: H₂ / Pd/C / ethyl acetate / 6 h / 760 Torr

2.2: 83 percent / aq. NaOH / methanol / 16 h / Heating

3.1: pyridine / CH₂Cl₂ / 1 h / 0 - 25 °C

3.2: oxalyl chloride; DMF / CH₂Cl₂ / 1 h / Heating

3.3: 65 percent / aq. Na₂CO₃ / diethyl ether; CH₂Cl₂ / 0.5 h

With pyridine; hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm0502135

Reference yield:

: 449779-66-2
methyl 2,4-dihydroxy-3,5-diallylbenzoate

: 449779-67-3
N-methyl-4-acetoxy-3,5-dipropyl-6-hydroxybenzohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd/C / ethyl acetate / 6 h / 760 Torr

1.2: 83 percent / aq. NaOH / methanol / 16 h / Heating

2.1: pyridine / CH₂Cl₂ / 1 h / 0 - 25 °C

2.2: oxalyl chloride; DMF / CH₂Cl₂ / 1 h / Heating

2.3: 65 percent / aq. Na₂CO₃ / diethyl ether; CH₂Cl₂ / 0.5 h

With pyridine; hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm0502135