N-[tris(pentafluorophenyl)borane]-pyridine

Base Information

Chemical Name:N-[tris(pentafluorophenyl)borane]-pyridine
CAS No.:2138-72-9
Molecular Formula:C₂₃H₅BF₁₅N
Molecular Weight:591.086
Hs Code.:

Synonyms:N-[tris(pentafluorophenyl)borane]-pyridine

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Chemical Property of N-[tris(pentafluorophenyl)borane]-pyridine

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Technology Process of N-[tris(pentafluorophenyl)borane]-pyridine

There total 23 articles about N-[tris(pentafluorophenyl)borane]-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-86-1
pyridine

: 1109-15-5
tris(pentafluorophenyl)borate

: 2138-72-9
N-[tris(pentafluorophenyl)borane]-pyridine

Guidance literature:: In dichloromethane; (N2); a soln. of ligand added at room temp. to a soln. of B(C6F5)3, stirred for 30 min at room temp.; evapd. (vac.);
DOI:10.1021/ic051285p

Reference yield: 72.0%

: 110-86-1
pyridine

: 914910-76-2
((CH₃)5C₅)Ta(CH₂C₆H₅)(C(CH₂C₆H₅)NC₆H₃(CH₃)2)OB(C₆F₅)3

: 2138-72-9
N-[tris(pentafluorophenyl)borane]-pyridine

: ((CH₃)5C₅)Ta(CH₂C₆H₅)(C(CH₂C₆H₅)NC₆H₃(CH₃)2)O

Guidance literature:: In toluene; under Ar, soln. of Ta compd. treated with py (1:1.5), stirred for 2 h atroom temp.; evapd., concd., pptd. (hexane), washed (hexane/toluene), elem. anal.;
DOI:10.1002/ejic.200500643

Reference yield: 71.0%

: 1001660-58-7
[(2-((2-OMe-Ph)2P)-4-Me-benzenesulfonate)Pd(pyridine)(CH₂SiMe₃)]

: 75-09-2
dichloromethane

: 1109-15-5
tris(pentafluorophenyl)borate

: 2138-72-9
N-[tris(pentafluorophenyl)borane]-pyridine

: [(2-((2-OMe-Ph)2P)-4-Me-benzenesulfonate)Pd(CH₂SiMe₃)]2*2CH₂Cl₂

Guidance literature:: In dichloromethane-d2; (N2); drybox or Schlenk technique; CD2Cl2 was vac. transferred to mixt. of Pd complex and B(C6F5)3 (1 equiv.) in NMR tube at -196°C; warmed to room temp. and agitated; maintained at 21°C for 12 h; solvent removed by syringe under N2; washed (pentane); dried (vac.); elem. anal.;
DOI:10.1021/om700869c