(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

Base Information

Chemical Name:(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride
CAS No.:473927-66-1
Molecular Formula:C₉H₁₁ClN₂O₃S
Molecular Weight:262.717
Hs Code.:

Synonyms:(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

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Chemical Property of (Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

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Technology Process of (Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

There total 2 articles about (Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 3-chloromethanesulphonyl acetone

: 104-94-9
4-methoxy-aniline

: 473927-66-1
(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; In water; acetone;

Reference yield: 57.0%

: 1-chloro-1-(methanesulfonyl)propan-2-one

: 104-94-9
4-methoxy-aniline

: 473927-66-1
(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

Guidance literature:: 4-methoxy-aniline; With hydrogenchloride; sodium nitrite; at -5 ℃; for 0.5h;

1-chloro-1-(methanesulfonyl)propan-2-one; With sodium acetate; In water; acetone; at 20 ℃; for 4h; Further stages.;
DOI:10.1021/jm070245n

Reference yield: 80.0%

: 473927-69-4
1-(4-iodo-phenyl)-3-morpholin-4-yl-5,6-dihydro-1H-pyridin-2-one

: 473927-66-1
(Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride

: 473927-67-2
6-(4-iodophenyl)-1-(4-methoxyphenyl)-3-(methylsulfonyl)-1,4,5,6-tetrahydro-7H-pyrazolo(3,4-c)pyridin-7-one

Guidance literature:: 1-(4-iodo-phenyl)-3-morpholin-4-yl-5,6-dihydro-1H-pyridin-2-one; (Z)-N'-(4-methoxyphenyl)-1-(methylsulfonyl)methanehydrazonoyl chloride; With triethylamine; In toluene; at 70 ℃; for 12h;

With hydrogenchloride; at 20 ℃; for 4h; Further stages.;
DOI:10.1021/jm070245n