picolinic acid 3-chlorobenzylamide

Base Information

Chemical Name:picolinic acid 3-chlorobenzylamide
CAS No.:1012972-76-7
Molecular Formula:C₁₃H₁₁ClN₂O
Molecular Weight:246.696
Hs Code.:

Synonyms:picolinic acid 3-chlorobenzylamide

Suppliers and Price of picolinic acid 3-chlorobenzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of picolinic acid 3-chlorobenzylamide

Chemical Property:

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Technology Process of picolinic acid 3-chlorobenzylamide

There total 2 articles about picolinic acid 3-chlorobenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-98-6
2-Picolinic acid

: 4152-90-3
m-chlorobenzylamine

: 1012972-76-7
picolinic acid 3-chlorobenzylamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/acs.joc.8b03098

Reference yield:

: C₁₁H₁₃NO₄

: 4152-90-3
m-chlorobenzylamine

: 1012972-76-7
picolinic acid 3-chlorobenzylamide

Guidance literature:: In tetrahydrofuran; at -15 - 20 ℃; Inert atmosphere;

Reference yield: 86.0%

: 1012972-76-7
picolinic acid 3-chlorobenzylamide

: 107-08-4
1-iodo-propane

: 1332481-64-7
C₁₆H₁₇ClN₂O

Guidance literature:: With oxygen; palladium diacetate; sodium triflate; potassium carbonate; In 3-methylpentan-3-ol; at 135 ℃; for 36h; under 760.051 Torr; regioselective reaction;
DOI:10.1021/ol201930e