3-Acetoxytricyclo[2.2.1.02,6]heptane

Base Information

Chemical Name:3-Acetoxytricyclo[2.2.1.02,6]heptane
CAS No.:6555-48-2
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:
Mol file:6555-48-2.mol

Synonyms:nortricycl-5-yl acetate;3-Nortricyclyl acetate;Tricyclo<2.2.1.02,6>heptan-3-ol-acetat;3-Acetoxynortricyclene;3-acetoxynortricyclane;

Suppliers and Price of 3-Acetoxytricyclo[2.2.1.02,6]heptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-Acetoxytricyclo[2.2.1.02,6]heptane

Chemical Property:

Vapor Pressure:0.226mmHg at 25°C
Boiling Point:207.4°C at 760 mmHg
Flash Point:70.1°C
PSA：26.30000
Density:1.19g/cm³
LogP:1.20390

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Acetoxytricyclo[2.2.1.02,6]heptane

There total 11 articles about 3-Acetoxytricyclo[2.2.1.02,6]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 528-76-7
2,4-dinitrobenzenesulfenyl chloride

: 64-19-7,77671-22-8
acetic acid

: 278-06-8
quadricyclo[2.2.1.0.0]heptane

: 6555-48-2,127057-06-1,127127-98-4,127127-99-5
3-acetoxynortricyclene

: 80698-18-6
Acetic acid (1R,2R,4S,5R,6R)-5-chloro-6-(2,4-dinitro-phenylsulfanyl)-bicyclo[2.2.1]hept-2-yl ester

: 66887-41-0
(1S,4R,5S,6S)-5-Chloro-6-(2,4-dinitro-phenylsulfanyl)-bicyclo[2.2.1]hept-2-ene

: 73464-48-9
(1S,3R,4R,5R)-3-Chloro-5-(2,4-dinitro-phenylsulfanyl)-tricyclo[2.2.1.0^2,6]heptane

Guidance literature:: at 20 ℃; for 2h; Further byproducts given;
DOI:10.1021/jo00347a018

Reference yield: 18.0%

: 528-76-7
2,4-dinitrobenzenesulfenyl chloride

: 64-19-7,77671-22-8
acetic acid

: 278-06-8
quadricyclo[2.2.1.0.0]heptane

: 6555-48-2,127057-06-1,127127-98-4,127127-99-5
3-acetoxynortricyclene

: 80698-20-0
Acetic acid (1R,2R,4R,5S)-5-acetoxy-7-(2,4-dinitro-phenylsulfanyl)-bicyclo[2.2.1]hept-2-yl ester

: 5257-37-4
(1RS,2SR,4RS)-bicyclo[2.2.1]hept-5-en-2-yl acetate

: 66965-67-1
Acetic acid (1R,3S,4S,5R)-5-(2,4-dinitro-phenylsulfanyl)-tricyclo[2.2.1.0^2,6]hept-3-yl ester

Guidance literature:: With lithium perchlorate; at 20 ℃; for 2h; Further byproducts given;
DOI:10.1021/jo00347a018

Reference yield: 17.0%

: 278-06-8
quadricyclo[2.2.1.0.0]heptane

: 6555-48-2,127127-98-4,127127-99-5
3-Acetoxynortricyclen

: 95596-80-8
nitrate of nortricyclan-3-ol

: nitrate of bicyclo<2.2.1>hept-3-ene-exo-1-ol

: 79150-84-8,95672-69-8
nitrate of 5-nitro-3-nortricyclanol

Guidance literature:: With acetyl nitrate; In acetic anhydride; Yield given. Further byproducts given. Yields of byproduct given; 1.)-15 to 0 deg C, 30 min 2.)10 deg C, 30 min;