N-(tert-butoxycarbonylmethyl)-4-butyramide

Base Information

• Chemical Name: N-(tert-butoxycarbonylmethyl)-4-butyramide
• CAS No.: 153957-98-3
• Molecular Formula: C₂₂H₂₆N₃O₁₀P
• Molecular Weight: 523.436

Synonyms:N-(tert-butoxycarbonylmethyl)-4-butyramide

Chemical Property of N-(tert-butoxycarbonylmethyl)-4-butyramide

Chemical Property:

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Technology Process of N-(tert-butoxycarbonylmethyl)-4-butyramide

There total 1 articles about N-(tert-butoxycarbonylmethyl)-4-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

Glycine tert-butyl ester (6456-74-2) + p-nitrophenyl 4-butyrate (129850-47-1) → N-(tert-butoxycarbonylmethyl)-4-butyramide (153957-98-3)

Guidance literature:

With dmap; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1055/s-1993-25982

Reference yield:

methanol (67-56-1) + N-(tert-butoxycarbonylmethyl)-4-butyramide (153957-98-3) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + {4-[Methoxy-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid tert-butyl ester

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; for 0.5h; Ambient temperature;

DOI:10.1055/s-1993-25982

Reference yield:

4-nitrobenzyl chloride (619-73-8) + N-(tert-butoxycarbonylmethyl)-4-butyramide (153957-98-3) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + {4-[(4-Nitro-benzyloxy)-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid tert-butyl ester

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1055/s-1993-25982

upstream raw materials:

Glycine tert-butyl ester

p-nitrophenyl 4-butyrate

Downstream raw materials:

4-nitro-phenol

{4-[Bis-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid

{4-[Methoxy-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid

N-(carboxymethyl)-4-butyramide

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