K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

Base Information

Chemical Name:K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA
CAS No.:1159806-63-9
Molecular Formula:C₄H₉NO*C₁₃H₂₈N₅NiO₃*K
Molecular Weight:487.307
Hs Code.:

Synonyms:K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

Suppliers and Price of K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

There total 1 articles about K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 1159806-92-4
bis[(N'-isopropylureido)-N-ethyl]-N-methylamine

: 7732-18-5
water

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: potassium hydride

: 1159806-63-9
K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

: 127-08-2
potassium acetate

Guidance literature:: In N,N-dimethyl acetamide; (Ar); treatment of soln. of urea deriv. in dimethylacetamide with 2 equiv. of KH at room temp., addn. of 1 equiv. of nickel compd. at room temp., filtration, addn. of 1 equiv. of KH, addn. of 1 equiv. of water; evapn., triturating with ether, isolation of ppt., IR and UV;
DOI:10.1039/b820209e

Reference yield: 94.0%

: 1159806-63-9
K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

: 10581-12-1
tetramethyl ammonium acetate

: 40949-94-8
potassium hexamethylsilazane

: [Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(oxo)]^(2-)

: [tetramethylammonium]0.5K_0.5[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(OSiMe₃)]*DMA

: 127-08-2
potassium acetate

Guidance literature:: In N,N-dimethyl acetamide; (Ar); treatment of soln. of nickel compd. in dimethylacetamide with 1 equiv. of potassium amide deriv. at room temp., stirring for 30 min, addn.of tetramethylammonium salt at room temp., stirring for 1 h; filtration, evapn., triturating with diethyl ether, isolation of ppt., recrystn. by diffusion of 1:1 diethyl ether/pentane vapour into soln. in dimethylacetamide, elem. anal.;
DOI:10.1039/b820209e

Reference yield: 91.0%

: 1159806-63-9
K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

: 865-47-4
potassium tert-butylate

: 10581-12-1
tetramethyl ammonium acetate

: [Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(oxo)]^(2-)

: 1159806-75-3
[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

: 127-08-2
potassium acetate

Guidance literature:: In N,N-dimethyl acetamide; (Ar); treatment of soln. of nickel compd. in dimethylacetamide with 1 equiv. of potassium tert-butoxide at room temp., stirring for 30 min, addn. of tetramethylammonium salt at room temp., stirring for 1 h; filtration, evapn., triturating with diethyl ether, isolation of ppt., recrystn. by diffusion of 1:1 ether/pentane vapour into soln. in dimethylacetamide, IR and UV;
DOI:10.1039/b820209e