[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

Base Information

Chemical Name:[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]
CAS No.:1159806-75-3
Molecular Formula:C₄H₁₂N*C₁₇H₃₆N₅NiO₃
Molecular Weight:491.341
Hs Code.:

Synonyms:[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

Suppliers and Price of [tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

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Technology Process of [tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

There total 2 articles about [tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1159806-92-4
bis[(N'-isopropylureido)-N-ethyl]-N-methylamine

: 865-47-4
potassium tert-butylate

: 10581-12-1
tetramethyl ammonium acetate

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: 1159806-75-3
[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

: 127-08-2
potassium acetate

Guidance literature:: With KH; In N,N-dimethyl acetamide; (vac. or Ar); treatment of soln. of urea deriv. in dimethylacetamide with KH, addn. of nickel compd., stirring for 45 min, addn. of potassium tert-butoxide, addn. of tetramethylammonium salt, stirring for 1 h; evapn. triturating with diethyl ether, isolation of ppt., elem. anal.;
DOI:10.1039/b820209e

Reference yield: 91.0%

: 1159806-63-9
K[Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(hydroxo)]*DMA

: 865-47-4
potassium tert-butylate

: 10581-12-1
tetramethyl ammonium acetate

: [Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(oxo)]^(2-)

: 1159806-75-3
[tetramethylammonium][Ni(bis[(N'-isopropylureido)-N-ethyl]-N-methylamine(-2H))(tert-butoxide)]

: 127-08-2
potassium acetate

Guidance literature:: In N,N-dimethyl acetamide; (Ar); treatment of soln. of nickel compd. in dimethylacetamide with 1 equiv. of potassium tert-butoxide at room temp., stirring for 30 min, addn. of tetramethylammonium salt at room temp., stirring for 1 h; filtration, evapn., triturating with diethyl ether, isolation of ppt., recrystn. by diffusion of 1:1 ether/pentane vapour into soln. in dimethylacetamide, IR and UV;
DOI:10.1039/b820209e