C₁₂H₇Cl₂F₃N₂O

Base Information

Chemical Name:C₁₂H₇Cl₂F₃N₂O
CAS No.:1033586-96-7
Molecular Formula:C₁₂H₇Cl₂F₃N₂O
Molecular Weight:323.102
Hs Code.:

C<sub>12</sub>H<sub>7</sub>Cl<sub>2</sub>F<sub>3</sub>N<sub>2</sub>O

Synonyms:C₁₂H₇Cl₂F₃N₂O

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Chemical Property of C₁₂H₇Cl₂F₃N₂O

Chemical Property:

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Technology Process of C₁₂H₇Cl₂F₃N₂O

There total 10 articles about C₁₂H₇Cl₂F₃N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033586-41-2
2-(1-(2-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)acetic acid

: 1033586-96-7
C₁₂H₇Cl₂F₃N₂O

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; for 0.5h;

Reference yield:

: 437711-25-6
1-(2-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid

: 1033586-96-7
C₁₂H₇Cl₂F₃N₂O

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

2: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -10 - 20 °C

3: dibromotriphenylphosphorane / dichloromethane / 2 h / 20 °C

4: N,N-dimethyl-formamide / 4 h / 50 °C

5: potassium hydroxide; ethanol / 17 h / Heating / reflux

6: hydrogenchloride / water; ethyl acetate

7: oxalyl dichloride / N,N-dimethyl-formamide / tetrahydrofuran / 0.5 h

With hydrogenchloride; dmap; potassium hydroxide; oxalyl dichloride; ethanol; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dibromotriphenylphosphorane; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 437711-24-5
1-(2-Chlorophenyl)-5-(2-furanyl)-3-(trifluoromethyl)-1H-pyrazole

: 1033586-96-7
C₁₂H₇Cl₂F₃N₂O

Guidance literature:: Multi-step reaction with 9 steps

1: sodium chlorite; sodium dihydrogenphosphate / water; acetonitrile / 42 h / 0 - 20 °C

2: hydrogenchloride / dichloromethane; water

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

4: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -10 - 20 °C

5: dibromotriphenylphosphorane / dichloromethane / 2 h / 20 °C

6: N,N-dimethyl-formamide / 4 h / 50 °C

7: potassium hydroxide; ethanol / 17 h / Heating / reflux

8: hydrogenchloride / water; ethyl acetate

9: oxalyl dichloride / N,N-dimethyl-formamide / tetrahydrofuran / 0.5 h

With hydrogenchloride; dmap; potassium hydroxide; sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; ethanol; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dibromotriphenylphosphorane; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;