acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

Base Information

Chemical Name:acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester
CAS No.:914490-51-0
Molecular Formula:C₁₇H₁₄F₃NO₃
Molecular Weight:337.298
Hs Code.:

Synonyms:acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

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Chemical Property of acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

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Technology Process of acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

There total 3 articles about acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 455-14-1
4-trifluoromethylphenylamine

: 65448-20-6
4-acetoxyphenylacetyl chloride

: 914490-51-0
acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 914490-51-0
acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 0.75 h / 80 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2.17 h / 0 - 20 °C

3: triethylamine / dichloromethane / 0.5 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; sulfuric acid; In dichloromethane;

Reference yield:

: 38177-33-2
(4-acetoxyphenyl)acetic acid

: 914490-51-0
acetic acid 4-[(4-trifluoromethyl-phenylcarbamoyl)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2.17 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0.5 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;