phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

Base Information

Chemical Name:phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate
CAS No.:1220707-90-3
Molecular Formula:C₂₄H₁₄ClF₃O₅S
Molecular Weight:506.886
Hs Code.:

Synonyms:phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

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Chemical Property of phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

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Technology Process of phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

There total 2 articles about phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1220707-81-2
phenyl 1,4-bis(trifluoromethylsulfonyloxy)-2-naphthoate

: 1679-18-1
4-Chlorophenylboronic acid

: 1220707-90-3
phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 95 ℃; for 8h; regioselective reaction;
DOI:10.1016/j.tetlet.2010.01.038

Reference yield:

: 54978-55-1
phenyl 1,4-dihydroxynaphthalene-2-carboxylate

: 1220707-90-3
phenyl 1-(4-chlorophenyl)-4-(trifluoromethylsulfonyloxy)-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 - 0 °C / Inert atmosphere

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 8 h / 95 °C / Inert atmosphere

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; 2.1: Suzuki coupling;
DOI:10.1055/s-0030-1260054