N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

Base Information

Chemical Name:N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester
CAS No.:1263914-10-8
Molecular Formula:C₂₅H₂₆NO₅P
Molecular Weight:451.459
Hs Code.:

Synonyms:N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

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Chemical Property of N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

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Technology Process of N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

There total 3 articles about N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1263913-86-5
(2-bromophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

: 122-52-1
triethyl phosphite

: 1263914-10-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

Guidance literature:: With palladium diacetate; at 160 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c0dt00881h

Reference yield:

: 615-36-1
2-bromoaniline

: 1263914-10-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: palladium diacetate / 1 h / 160 °C / Inert atmosphere

With pyridine; palladium diacetate; In dichloromethane;
DOI:10.1039/c0dt00881h

Reference yield:

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1263914-10-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-2-aminophenylphosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: palladium diacetate / 1 h / 160 °C / Inert atmosphere

With pyridine; palladium diacetate; In dichloromethane;
DOI:10.1039/c0dt00881h