2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt

Base Information

• Chemical Name: 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt
• CAS No.: 70317-21-4
• Molecular Formula: C₂H₆F₈N₂P₂*2H
• Molecular Weight: 274.034
• Mol file: 70317-21-4.mol

Synonyms:2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt

Chemical Property of 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt

There total 4 articles about 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ⁶,4λ⁶-diazadiphosphetidin-HF-Addukt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2,2,2,4,4,4-hexafluoro-1,3-dimethyl-1,3,2λ5,4λ5-diazadiphosphetidine (3880-04-4) + phenylhydrazine (100-63-0) → 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ6,4λ6-diazadiphosphetidin-HF-Addukt (70317-21-4) + 2,2,2,4,4-Pentafluor-1,3-dimethyl-4-(N2-phenylhydrazino)-1,3,2λ5,4λ5-diazadiphosphetidin-HF-Addukt + 2,2,4,4-Tetrafluor-1,3-dimethyl-2,4-bis-(N2-phenylhydrazino)-1,3,2λ5,4λ5-diazadiphosphetidin

Guidance literature:

In benzene; for 4h; Ambient temperature;

DOI:10.1007/BF00810086

Reference yield: 81.0%

2,2,2,4,4,4-hexafluoro-1,3-dimethyl-1,3,2λ5,4λ5-diazadiphosphetidine (3880-04-4) + cyclohexanol (108-93-0) → 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ6,4λ6-diazadiphosphetidin-HF-Addukt (70317-21-4) + 2-Cyclohexyloxy-2,2,4,4,4-pentafluoro-1,3-dimethyl-2λ5,4λ5-[1,3,2,4]diazadiphosphetidine (94446-23-8)

Guidance literature:

In dichloromethane; for 12h; Yields of byproduct given; Ambient temperature;

DOI:10.1007/BF00798756

Reference yield: 80.0%

2,2,2,4,4,4-hexafluoro-1,3-dimethyl-1,3,2λ5,4λ5-diazadiphosphetidine (3880-04-4) + aniline (62-53-3) → 2,2,2,4,4,4,4-Octafluor-1,3-dimethyl-1,3,2λ6,4λ6-diazadiphosphetidin-HF-Addukt (70317-21-4) + (2,2,4,4,4-Pentafluoro-1,3-dimethyl-2λ5,4λ5-[1,3,2,4]diazadiphosphetidin-2-yl)-phenyl-amine (107426-29-9)

Guidance literature:

In dichloromethane;

DOI:10.1007/BF00816522

upstream raw materials:

2,2,2,4,4,4-hexafluoro-1,3-dimethyl-1,3,2λ⁵,4λ⁵-diazadiphosphetidine

aniline

phenylhydrazine

cyclohexanol

Downstream raw materials:

2,2,4,4-Tetrafluor-1,3-dimethyl-2,4-diphenyl-1,3-diaza-2,4-diphospha-cyclobutan

2,2,2,4,4,4-hexafluoro-1,3-dimethyl-1,3,2λ⁵,4λ⁵-diazadiphosphetidine