(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Base Information

Chemical Name:(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane
CAS No.:149228-92-2
Molecular Formula:C₁₄H₂₃BrOSi
Molecular Weight:315.326
Hs Code.:

Synonyms:(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Suppliers and Price of (4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

There total 2 articles about (4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7463-51-6
4-bromo-3,5-dimethylphenol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 149228-92-2
(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1055/s-2006-950313

Reference yield: 97.0%

: 149228-92-2
(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

Guidance literature:

Reference yield: 90.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 149228-92-2
(4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane

: 378185-89-8
4-(tert-butyldimethylsilanyloxy)-2,6-dimethylbenzaldehyde

Guidance literature:: (4-bromo-3,5-dimethylphenoxy)(tert-butyl)-di-methylsilane; With methyllithium; lithium bromide; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.0833333h;

With sec.-butyllithium; In tetrahydrofuran; diethyl ether; cyclohexane; at -78 ℃; for 0.0833333h;

N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; cyclohexane; at -78 - 20 ℃; Further stages.;
DOI:10.1080/00304940709356013