N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

Base Information

Chemical Name:N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide
CAS No.:918401-81-7
Molecular Formula:C₁₅H₁₉ClFNO₄S
Molecular Weight:363.838
Hs Code.:

Synonyms:N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

Suppliers and Price of N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

There total 1 articles about N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 110-57-6
trans-1,4-dichlorobut-2-ene

: 501682-72-0
N-(tert-butyloxycarbonyl)-4-fluorobenzenesulfonamide

: 918401-81-7
N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; for 16h; Heating;
DOI:10.1039/b608673j

Reference yield: 90.0%

: 918401-81-7
N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

: 402-46-0
4-fluorophenylsulphonamide

: 850334-72-4
(E,E)-1,11-bis(tert-butyloxycarbonyl)-1,6,11-tris[(4-fluorophenyl)sulfonyl]-1,6,11-triazaundeca-3,8-diene

Guidance literature:: With potassium carbonate; In acetonitrile; for 7h; Heating;
DOI:10.1039/b608673j

Reference yield:

: 918401-81-7
N-[(E)-4-chloro-2-buten-1-yl]-N-(tert-butoxycarbonyl)-(4-fluorophenyl)sulfonamide

: 918401-72-6
1,6,11-tris[(4-fluorophenyl)sulfonyl]-1,6,11-triazacyclopentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / potassium carbonate / acetonitrile / 7 h / Heating

2: 80 percent / trifluoroacetic acid / CH₂Cl₂ / 5 h

3: 70 percent / potassium carbonate / acetonitrile; tetrahydrofuran / 3 h / Heating

4: 93 percent / H₂ / Pd/C; platinum(IV) oxide monohydrate / 2 h / 20 °C / atmospheric pressure

With hydrogen; potassium carbonate; trifluoroacetic acid; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/b608673j