Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)

Base Information

• Chemical Name: Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)
• CAS No.: 138497-36-6
• Molecular Formula: C₂₇H₂₁Cl₆MnN₄O₃
• Molecular Weight: 717.145
• Mol file: 138497-36-6.mol

Synonyms:Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)

Chemical Property of Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)

Chemical Property:

Purity/Quality:

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Technology Process of Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)

There total 1 articles about Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

tetra-n-butylammonium permanganate (35638-41-6) + tris{2-[(3,5-dichlorosalicylidene)amino]ethyl}amine (70292-82-9) + manganese (II) acetate tetrahydrate (6156-78-1) → Mn(N(CH2CH2NCHC6H2(3,5-Cl2)O)3) (138497-36-6)

Guidance literature:

In ethanol; addn. of solid Mn(OAc)2*4H2O to a soln. of the ligand in hot ethanol; stirring at 330 K for 15 min; addn. of (NBu4)MnO4 in portions; stirring for 0.5 h;; removal of solvent under vac.; dissoln. in DMF; filtration; slow evapn. of filtrate at room temp.; the ppt. was filtered off and dried in air; recrystn. from DMF; elem. anal.;

DOI:10.1039/DT9910002917

upstream raw materials:

tetra-n-butylammonium permanganate

tris{2-[(3,5-dichlorosalicylidene)amino]ethyl}amine

manganese (II) acetate tetrahydrate