N-(2,4-Dinitrophenyl)ethylenediamine

Base Information

• Chemical Name: N-(2,4-Dinitrophenyl)ethylenediamine
• CAS No.: 28767-75-1
• Molecular Formula: C8H10N4O4
• Molecular Weight: 226.192
• Hs Code.: 2921590090
• European Community (EC) Number: 673-476-6
• DSSTox Substance ID: DTXSID30182949
• Nikkaji Number: J1.297.045E
• Wikidata: Q83053680
• Mol file: 28767-75-1.mol

Synonyms:DNPED;N-(2,4-dinitrophenyl)ethylenediamine

Chemical Property of N-(2,4-Dinitrophenyl)ethylenediamine

Chemical Property:

• Vapor Pressure: 1.38E-07mmHg at 25°C
• Refractive Index: 1.67
• Boiling Point: 429.6 °C at 760 mmHg
• Flash Point: 213.6 °C
• PSA: 129.69000
• Density: 1.48 g/cm³
• LogP: 2.69330
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 226.07020481
• Heavy Atom Count: 16
• Complexity: 262

Purity/Quality:

97% ^*data from raw suppliers

N1-(2,4-Dinitrophenyl)ethane-1,2-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])NCCN
• Uses: N1-(2,4-Dinitrophenyl)ethane-1,2-diamine is a useful chemical reagent.

Technology Process of N-(2,4-Dinitrophenyl)ethylenediamine

There total 12 articles about N-(2,4-Dinitrophenyl)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C13H18N4O6 (911209-11-5) → N1-(2,4-dinitrophenyl)ethane-1,2-diamine (28767-75-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 90.0%

5-amino-1-(2,4-dinitrophenyl)-1H-pyrazole-4-carbonitrile (75008-95-6) + ethylenediamine (107-15-3,85404-18-8) → N1-(2,4-dinitrophenyl)ethane-1,2-diamine (28767-75-1)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.3184/030823408X338693

Reference yield: 60.0%

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + ethylenediamine (107-15-3,85404-18-8) → N1-(2,4-dinitrophenyl)ethane-1,2-diamine (28767-75-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

upstream raw materials:

ethylenediamine

1-chloro-2,4-dinitro-benzene

2,4-Dinitrofluorobenzene

7-phenyl hexahydro-1,4-diazepine-5-one

Downstream raw materials:

tert-butyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoate

N-(2-(2,4-dinitrophenylamino)ethyl)acetamide

3',5'-di-O-acetyl-2'-deoxy-N₂-{2-[(2,4-dinitrophenyl)amino]ethyl}-O₆-[2-(4-nitrophenyl)ethyl]guanosine

C₁₁H₁₅N₄O₇P

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